By Leo A. Paquette
There are various books on hand in regards to the chemistry and biology of sulfur. notwithstanding, this can be the 1st booklet with a compilation of all proper Sulfur containing reagents. man made chemists, such a lot rather within the medicinal and pharmaceutical chemists, are usually referred to as upon to arrange compounds that comprise Sulfur as a key structural function. long ago, this a website for experts; at the present time each man made chemist operating in those zone is anticipated to synthesize compounds containing sulfides, sulfates, sulfones, and so forth. This booklet deals a big resource of data for the choice and dealing with of definitely the right reagents.
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Extra info for Handbook of Reagents for Organic Synthesis, Sulfur-Containing Reagents
Stadnichuk, M. ; Kryukova, T. ; Petrov, A. , Zh. Obshch. Khim. 1975, 45, 838. Vasin, V. ; Bolusheva, I. ; Chernyaeva, L. ; Tanaseichuk, B. ; Surmina, L. ; Zeﬁrov, N. , Zh. Org. Khim. 1990, 26, 1509. , Chem. Ber. 1976, 109, 2315. CF3O3S/h89H;/q+1;-1 InChIKey = IWYHWZTYVNIDAE-ZJHSAWQHCT (example of a series of closely related reagents serving as promoters for condensation of a nucleoside phosphoramidite and a nucleoside/nucleotide, constructing internucleotide linkage1−5 ) Physical Data: mp 188–190 ◦ C; density unknown.
23 O S N 1. MeOTf, MeNO2 2. NaBPh4 1 OMe OMe O OBn O B O O BnO S O HO 1, Tf2O, TTBP BPh4 (10) CO2Et (11) O 32 27 CH2Cl2, −60 °C B O O BnO O SPh 26 CO2Et OMe OBn O O 2. 32 H2O, Me2CO O O 1. NaH, DME 33 Δ OMe O O 28 OBn O HO HO BnO CO2Et OMe O O O Me (8) Related Reagents. 1 The standard BSP/Tf2 O/TTBP reagent combination activates selenoglycosides in a manner analogous to thioglycosides. 1 O O BnO + 34 O 29 Ph N 1. , J. Am. Chem. Soc. 2001, 123, 9015. 2. , Org. Lett. 2000, 2, 4067. 3. , Synthesis 2001, 323.
Stachel, S. , Tetrahedron Lett. 1993, 34, 6209. (l) Bregant, T. ; Little, R. , J. Am. Chem. Soc. 1994, 116, 3635. (m) Ott, G. ; Heathcock, C. , Org. Lett. 1999, 1, 1475. ; Vicic, D. ; McIntosh, M. , Org. Lett. 2003, 5, 1039. (o) Sammis, G. ; Flamme, E. ; Ho, D. ; Sorensen, E. , J. Am. Chem. Soc. 2005, 127, 8612. Myers, A. , Tetrahedron Lett. 1996, 37, 4841. ; Siegel, D. , Angew. , Int. Ed. 2006, 45, 5859. Myers, A. , J. Am. Chem. Soc. 1997, 119, 8572. (mild sulfonating agent; useful for the preparation of sulfonamides, sulfones, and sulfonate esters) Physical Data: mp 65–80 ◦ C; 88–91 ◦ C after recrystallization from ether.